ELOG 8-ID

8-ID-D pogo stick upgrade review material - Nov. 7, 2005

Safety

Material presented to the Beamline Safety Design Review Steering Committee (BSDRSC) on Nov. 7, 2005. Attachments include Soon Hong's and Michael's presentations.

Attachment 1: D_station_monochromator_upgrade.ppt

Attachment 2: Design_Review_D_monochromator_Soon_Hong.pdf

104

Thu Sep 7 10:35:58 2006

Michael

8-ID-D pogo stick upgrade review material - Nov. 7, 2005

Safety

Approval from the BSDRSC (attached)

Quote:

Material presented to the Beamline Safety Design Review Steering Committee (BSDRSC) on Nov. 7, 2005. Attachments include Soon Hong's and Michael's presentations.

Attachment 1: TN05-033_Closeout.pdf

416

Wed Apr 8 23:23:03 2015

8-ID-E Beamline characterization on 4/8/2015

Hi all,

I hosted Xianbo Shi, Nick Sereno, and Yianbo today.
I set up a GaAs edge for 8-ID-E and we used it to
bissect the beam in the focal plane of the CXRL in 8-ID-E.

The measurements were a bit delayed because I found the flux
had dropped from 3 to 1.7 x 10^9 ph/s since last Wednesday.
This is after realigning the beamline. I also wasn't ready for them
as I had to hunt for cables, patch panels, and mounts for the GaAs edge.

Anyhow, the technique we used is easy to reproduce.
The flux is measured with a calibrated PIN diode from the detector pool (28x28 mm).
We teed off the voltage from the SR-570 and sent one output to
a 500 MHz digital scope. I glued a GaAs knife edge and mounted it on a goniometer.
The beam was bissected in the horizontal or vertical direction.
Att. 1 shows the focal spot size (6 microns). Att. 2 shows ray traces
including diffraction performed by Ruben Reininger in January 2015.
They are consistent with today's experimental conditions.
The RMS spot size is expected to be 2.1 microns, so the FWHM should be 5 microns.
We measure 6, but it was a kluggy measurement.

I am expecting a report that will be posted.
We investigated sources of noise, including a roughing pump,
and the 2nd crystal turbopump. Then we removed the lens from the
beam path. If the lens mount vibrate, it could broaden the focal spot
and steer the beam with vibration.

This is a preliminary report that will be updated.
They thought the beamline was pretty quiet, and noted some frequencies around 78 Hz.

ED

Date: Fri, 5 Jun 2015 16:34:15 -0500
From: Eric Dufresne <[email protected]>
To: "Shi, Yingbo" <[email protected]>
Cc: "Reininger, Ruben" <[email protected]>,
"Shi, Xianbo" <[email protected]>, Alec Sandy <[email protected]>
Subject: Re: beamline measurement

Yingbo,

Alec Sandy filled out the tab on the 8IDEXPCS set up.
https://anl.app.box.com/files/0/f/2978874453/8_ID_E (I attached the May 22, 2015 version)

Note that we measured the vertical focal spot size at 0.006 mm.

Have a good weekend,
Eric

P.S. Why is Yingbo's email bouncing? Maybe it was a temporary thing...

Attachment 1: lineup040815-scan20.png

Attachment 2: CRLfocusing-8IDE-7350eV-1D.png

Attachment 3: 8IDE_May2015.xlsx

591

Fri Sep 21 12:24:41 2018

8-ID-E Lakeshore 340 connection and settings for Oleg's cryostat

Controls

For the 8-ID-E, the lakeshore 340 used by Oleg uses asyn 2.
It requiires a RJ-11 to D9 adapter described earlier in
https://8id.xray.aps.anl.gov/elog/8-ID/503 (Lakeshore model 117-020)
and a straight through D9 to RJ-45 connector.
RJ-45 D9
2--------2
3--------3
4--------4
5--------5
6--------7

I provide in att. 1 the pinout of the L-com RA098M connector.
from http://www.l-com.com/ethernet-modular-adapter-db9-male-rj45-8x8-jack

To check the communication, you type the command in the image below
https://8id.xray.aps.anl.gov/elog/8-ID/503/1

Worthy references

https://8id.xray.aps.anl.gov/elog/8-ID/305 Joe and communication parameters
https://8id.xray.aps.anl.gov/elog/8-ID/288 Manual (Suresh) p124 for commands
https://8id.xray.aps.anl.gov/elog/8-ID/588 UCSD cryostat manual and drawings
https://8id.xray.aps.anl.gov/elog/8-ID/390 To change heater resistance (50 Ohm)
Lakeshore PID parameters for heater at 1A in att. 3
Lakeshore PID parameters for heater at 333mA in att. 4

Attachment 1: RA098M.pdf

Attachment 2: 0711_001.pdf

Attachment 3: Lakeshore1A.png

Attachment 4: Lakeshore340-More-072820.png

236

Mon Jul 27 14:02:31 2009

J. F. Pelletier (posted by Joe)

8-ID-E Layout information from IMMY-XOR webpage

Other

The attached information about the layout of the 8-ID-E hutch was previously posted on the IMMY-XOR webpage under User Info/Layout/Sector 8

8-ID XOR - Layout

8-ID XOR 8-ID-E Hutch

Hutch 8-ID-E provides monochromatic X-rays to two experimental setups on a side station using a
transmission diamond monochromator.

The currently installed experimental setups are the TRXS spectrometer and the large horizontal
spectrometer. They are sitting one behind the other, as shown in the hutch layout below, and use
X-rays from either the first or third undulator harmonic at 7.66 keV or 23.0 keV respectively.

DWG (244K) EPS (304K) Hutch layout

Some pictures:

Construction 1997
Outside
Inside
Setups currently installed

J. F. Pelletier
June 2000

Attachment 1: 8-ID-E_XOR_-_Layout.mht

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... 583 more lines ...

Attachment 2: 8IDE_layout.dwg

Attachment 3: 8IDE_layout.ps

Attachment 4: hutch1.jpg

Attachment 5: 8id-e-2.jpg

Attachment 6: 8id-e-1.jpg

Attachment 7: trxs_hs01.jpg

665

Mon Aug 19 16:45:20 2019

Beamline 8-ID-E operates with a single-bounce monochromator, and therefore at fixed operating energy.
Since June 2016, all experiments on 8-ID-G (Grazing Incidence instrument) have operated at 10.9 keV provided by the Si(111) crystal.
Since June 2016, all experiments on 8-ID-E (WA-XPCS instrument) have operated at 7.35 keV provided by the Si(220) crystal.

Prior to June 2016, the Grazing Incidence instrument on 8-ID-G was setup at a different angle and operated at 7.35 keV, provided by the Si(111) crystal.

For information on the Reflectivity curves of the monochromator crystals, see entry 653/mirror 653

P.S. 10/30/2019

On Oct 21, I took a picture of the monochromator for operation of Si (220) at 7.35 keV.
Note the painting tape with the Si (220) marks. This was prior to aligning the beam on 10/22 but should be close.
I took this picture as a reference in case we loose the motor position.
I am amazed how well this monochromator has worked frankly since 2014 but you never know.
ED

Attachment 1: 20191021_153953.jpg

364

Tue May 27 16:38:48 2014

8-ID-E O. Shpyrko cryostat mount pictures

Sample Environments

/home/beams/DUFRESNE//8ID/8ID-E/Cryostats/Shpyrko-2014 also has drawings from Alec.

I put additional material on my Experiments web page
so http://7id.xray.aps.anl.gov/~dufresne/Experiments/8ID/Cryostat-ST500/

ED

Attachment 1: IMAG1104.jpg

Attachment 2: IMAG1105.jpg

758

Wed Dec 16 13:55:12 2020

Joe Strzalka

8-ID-E instrument computer pepper

Computers and Network

2020.12.07 The Linux machine interfaced with the GIXS and WA-XPCS instruments, pepper, and its video card
were identified as insufficient for supporting remote access via NXwebplayer. Replacements have been ordered via AMOS:

AMOS Master Order number: 588501
SMART BUY Z4 G4 WKSTN XW2123 8GB 256GB SSD DVDRW W10P 64BIT
AXIOM 8GB DDR4-2666 ECC RDIMM FOR HP - 1XD84AA 1XD84AT --- 3 pieces
AMOS Master Order number: 588502
HP QUADRO P2200 GRAPHIC CARD - 5 GB - DISPLAYPORT from MNJ

2020.12.16 the RAM has been received and is in an envelope in the bin on my office door.

When the computer and video card arrive, we need to ask Jeff or Troy to set up the new machine and swap it for the current pepper.
Probably we will excess the old pepper.

From: Strzalka, Joe <[email protected]>
Sent: Monday, December 7, 2020 04:48 PM
To: Narayanan, Suresh <[email protected]>; Dufresne, Eric <[email protected]>
Cc: Lutes, Troy E. <[email protected]>; Hoffman, Jeff S <[email protected]>
Subject: NX remote access discussion session

Hi Suresh,

I�m attending the 2nd option for the remote access discussion with John Hammonds. Zhan Zhang was describing difficulty
seeing the cursor in remote access, and they thought it was due to their old NVidia video card and old computer.
We also have issues with cursor becoming invisible sometimes, especially for ImageJ. Troy was also attending,
and looked at the specs on pepper. He says pepper and our nvidia card do not meet the specs for remote access
via NX, and should be upgraded to newer equipment.

Troy, can you recommend a replacement machine/card for us?

Thank you,

Joe

P.S. We got a Z4 with 32 GB memory

Attachment 1: ScreenShot-Z4-Memorry2020-12-08at10h21m38AM.png

819

Tue Nov 16 14:54:03 2021

8-ID-E optical table 2 pictures

Drawings

https://anl.box.com/s/ue1hdki7oht6byrjirjaonfyzjd2cngj

From: Dufresne, Eric <[email protected]>
Sent: Tuesday, November 16, 2021 2:27 PM
To: Capatina, Dana <[email protected]>; Wakefield, Kevin J <[email protected]>
Cc: Fisher, Mike V. <[email protected]>; Narayanan, Suresh <[email protected]>; Sandy, Alec R. <[email protected]>
Ziegler, Raymond <[email protected]>; Highland, Matthew J. <[email protected]>
Subject: Re: XPCS team meeting - Wed, 3pm

This is a meeting's follow up, Dana and Kevin.
I took pictures on the 8-ID-E WA-XPCS optical table.
My experience has been good with the jacks on this table.
I will typically scan it in X+Y on a 20 um focused beam to center
it on my 60 um guard slits. It is a 6'x4'x1' table and I was able to get the drawing numbers
for the 3 vertical jacks, and one horizontal motorized slide.
I am missing the other two horizontal slides, one is motorized,
while the other is just a slide. Looking at EPICS screens, it looks like
it has a Z slide as well. Will have to get back to you on this has I don't have access
to the hutch right now, the 8ID-G robot is being tested...

https://anl.box.com/s/ue1hdki7oht6byrjirjaonfyzjd2cngj

It is a table purchased by MIT built by AJR, big round vertical jacks.

Eric

From: Dufresne, Eric <[email protected]>
Date: Tuesday, November 16, 2021 at 2:43 PM
To: Capatina, Dana <[email protected]>, Wakefield, Kevin J <[email protected]>
Cc: Fisher, Mike V. <[email protected]>, Narayanan, Suresh <[email protected]>, Sandy, Alec R. <[email protected]>,
Ziegler, Raymond <[email protected]>, Highland, Matthew J. <[email protected]>
Subject: Re: XPCS team meeting - Wed, 3pm

The first few pictures actually show the Z stage, they are with the vertical jack S/N 048,
so this foot has XYZ, the table has 6 motorized stages.

ED

Re: XPCS team meeting - Wed, 3pm
Sandy, Alec R. <[email protected]>
Tue 11/16/2021 3:05 PM
To: Narayanan, Suresh <[email protected]>; Dufresne, Eric <[email protected]>; Capatina, Dana <[email protected]>;
Wakefield, Kevin J <[email protected]>
Cc: Fisher, Mike V. <[email protected]>; Ziegler, Raymond <[email protected]>; Highland, Matthew J. <[email protected]>

Hi,

The stages and base frame are from a goniometer support assembly from the APS beamline design library from the early-mid 90s.
Can�t remember if it is T6-25 or T6-29 � something like that. There would be paper drawings in the file cabinet in the back
hallway. The motorized slides and followers are by design so that the motions are not over constrained and so the full
EPICS table record can be used. Deming will know all about these.

- Alec

Re: XPCS team meeting - Wed, 3pm
Dufresne, Eric <[email protected]>
Tue 11/16/2021 6:00 PM
To: Capatina, Dana <[email protected]>; Wakefield, Kevin J <[email protected]>
Cc: Fisher, Mike V. <[email protected]>; Ziegler, Raymond <[email protected]>;
Highland, Matthew J. <[email protected]>; Narayanan, Suresh <[email protected]>; Sandy, Alec R. <[email protected]>

Dana, Kevin,

I updated the link below with several pictures taken today, showing
the Z slide a bit more, the Y slides limits status, the manual jack and the feet
positions (Alec reminded me about these: they are low, thanks Alec), the footprint (thanks Suresh).
https://anl.box.com/s/ue1hdki7oht6byrjirjaonfyzjd2cngj

https://anl.box.com/s/r13euz3hniehq7wvlc44wde7l7vcbnx0
This is the approximate footprint, my note on table height (~1.04m), status of
vertical jacks (about 35 mm above lower limit), and travel range.

Learned to interrupt the robot too.

There is a classic SRI ~1995-1996 paper that describes these design by Deming.
We would find what Alec mentioned earlier. This is a classic of old APS designs.

Eric

620

Tue Feb 5 10:53:35 2019

Open Chathoth's chamber to higher angles and check reflectivity heater for high temperature operation (done!)
Check JJ x-ray encoder
Clean up EPICS, remove sg1 in slits both in epics and spec
remove pind1, rename pinds appropriately
Get Huber pin spacer/IUCR mount
Order more TL stuff
Tune PID on Lakeshore for cryostat when 1A current
Check samz limit. Must be switched.
Document drawings for 8-ID-E

756

Wed Dec 9 23:44:06 2020

The Fast Shutter for the GIXS instrument is a Cedrat fast shutter, installed 09 Dec 2020. It is located downstream of the intensity monitor pind1 and upstream of the filter banks.

During an interim period, the instrument used a thick foil on the 2nd filter bank, XIA2, Filter 3 as a temporary fix (20-24 Nov 2020).

Prior to that, since at least Nov 2008, the fast shutter was by AZsol.

Entries on the Cedrat shutter:
Documentation and installation notes (first installation on WA-XPCS by Eric Dufresne): entry 657 /mirror 657
The rack 12044 drives the FPS400M S/N 18002, installed in 8ID-G.

https://anl.box.com/s/6xrpb3ukjy0r50rit541ysid0xta8bm6 Pictures of installation.
Note the black soot on the upstream side of the old shutter. Likely cracked hydrocarbons from x-rays.

319

Thu Mar 29 10:32:41 2012

Joe Strzalka

8-ID-G GISAXS vacuum controller and vacuum system

Beamline Hardware

Cycle 2012-2, 2012.03.29

For about two weeks now, the upstream vacuum pump has been replaced temporarily because the roughing pump on the unit failed.

Today, the roughing pump on the downstream turbo pump unit appears to have died.
Symptoms:
1. Yesterday, odor from pump (oil or hot insulation smell)
2. Today, turbo pump not reaching full rotation spped (1000 Hz )

Temporary work around:
Enter emergency stop (E-Stop) on vacuum controller. Enter administrative mode and 'Pump all' so roughing pump pumps on downstream flight path. Turbo pump maxed out at only 730 Hz. After touchscreen showed "Good Vacuum" upstream sample and downstream, the upstream gate valve still did not open. Needed to increase the setpoint 4 (vacuum gauge at exit window of downstream flight path) to 3 x 10^0 (above the pressure reading of 2.7 x 10^0). After upstream gatevalve opened, vacuum at turbo pump improved and speed reached > 900 Hz, but not 1000 Hz. Users looked at a couple samples, plan is for Ray to swap out parts on the roughing pump and see if perfromacne improves.

Attachment: pdf powerpoint file with notes on the vacuum system.

Attachment 1: VacuumSystem8IDG.pdf

494

Fri Jan 27 15:59:20 2017

This entry serves as a stub for a User Manual for GIXS Users at Beamline 8-ID-G. The idea is to provide a place for links to other Elog entries for specific topics.Offsite users should follow the mirror links. The regular entries are not accessible offsite.

.A. Upstream Optics
.......1. White Beam Slits in A-Station
.......2. D-Station Monochromator entry 665/mirror 665
.B. E-Hutch (Hardware)
.......1. Upstream components
............a. XIA Filters entry 465/mirror 465
............b. Fast shutter entry 756/ mirror 756
............c. Be CRL for vertical focus entry 556/mirror 556
.......2. Diffractometer
............a. Calibration information: entry 397/ mirror 397
.......3. Sample Environments
............a. Multi-sample Vacuum Environment for static measurements with automated sample changer entry 696/mirror 696
............b. Solvent Vapor Annealing entry 669/mirror 669
............c. Relative Humidity entry 669/mirror 669
..................i. Humidity sensor HC-610 from Ohmic Instruments: attachments 3-5 of entry 411/mirror 411.
............d. Filmetrics F20-UV for in situ thickness monitoring via spectral reflectance: Filmetrics support page
............e. Thermal Annealing
..................i. Linkam HFSX350-GI Stage:
........................(1) Part 1 entry 540/mirror 540
........................(2) Part 2 entry 560/mirror 560
........................(3) Part 3 entry 561/mirror 561
........................(4) Part 4 entry 578/mirror 578 expansion board for serial communications
.................ii. Lakeshore 340 Unit manual: entry 288/ mirror 288
................iii. High temperature (700 C) oven
........................(1) Setup and operations: entry 351/mirror 351
.................iv. Thermal grease: entry 673/mirror 673
............f. In situ charge transport measurements entry 696/mirror 696 (see attachments)
...................i. Keithley 2400 Source-Meter SMU Instrument -- vendor site with links to manual and spec sheet
..................ii. Keithley 2400 at the beamline and EPICS support entry 528/ mirror 528
.................iii. Keithley 2400 for sweep scans with modified IOC to support waveform output entry 609/ mirror 609
..................iv. Keithley 2450 sourcemeter for 9-ID-D: entry 873 / mirror 873
............g. Inert atmosphere
...................i. Oxygen sensor
............h. Tensile stage entry 579/ mirror 579
............i. Agilent 33522A function generator support entry 648/ mirror 648
............j. Mini breadboard plates entry 650/ mirror 650
............k. Optical components: alignment laser entry 651/ mirror 651
............l. Spin coater
.......4. Downstream components
............a. Detector table: 3-D model accessible in Creo with the name �4308-460000.asm�
............b. Secondary detector system entry 702/ mirror 702
.......5. Detector
..............a. Pilatus 1M
..............b.
.C. E-Station (Software and Controls)
......-1. Beamline computer: pepper entry 762/ mirror 762
.......0. Remote user access via NX client entry 731/ mirror 731
.......1. EPICS, caQtDM/MEDM and Spec:
..............a. Starting up EPICS and Spec and Pilatus interfaces
....................i. caQtDM (2018-1-present)entry 566/mirror 566
...................ii. medm (up to 2017-3) entry 495/mirror 495
..............b. Useful description of Spec and EPICS from 7-ID https://www1.aps.anl.gov/Sector-7/7-ID/Beamline-Controls-and-Data-Handling
..............c. Writing macros in Spec at 8-ID-E entry 685/entry 685
.......2. Matlab entry 496/mirror 496
.......3. GIXSGUI
............a. download: https://www.aps.anl.gov/Sector-8/8-ID/Operations-and-Schedules/Useful-Links/Sector-8-GIXSGUI
............b. GIXSGUI helpfile: https://www.aps.anl.gov/files/download/SECTOR8/8-ID/doc.pdf
............c. Manual for fitting curves in GIXSGUI: linefit_manual.pdf
............d. Help getting started with GIXSGUI and FAQ list: entry 612/mirror 612
.......4. Pepper screen configuration: entry 575/mirror 575
.D. Chemistry Lab: entry 829/mirror 829
.E. Mechanical Lab
.F. Polymer Lab (spin coater): entry 226/mirror 226
.G. Remote Data Access
......1. PVwebmonitor: entry 553/mirror 553
......2. Live Specplots: entry 554/mirror 554
.H. Documents
......1. Sector Orientation entry 536/mirror 536
......2. Tip sheets
.............a. Vacuum GISAXS and GIWAXS with the multi-sample chamber entry 497/mirror 497
......3. ESAF materials
.............a. Experimental Safety Overview
.............b. General ESAF instructions entry 589/mirror 589
.............c. Standard Operating Procedures
....................1. Carcinogens: entry 555/mirror 555
....................2. Linkam stage/Cryogens: entry 639/mirror 639
....................3. Use of the spin coater in the Polymer Lab: entry 226/mirror 226
....................4. Venting the GIXS Beamline Safely: entry 754/ entry 754
......4. Bringing samples and other materials to Argonne
.............a. Transporting hazardous materials to the APS
.............b. DOT small quantities exceptions
......5. Chemical Waste Instructions, Log Sheet and Example: entry 672/mirror 672
......6. docs8ide -- GitHub-based documentation for 8-ID-E: entry 767/ mirror 767
.I. User FAQs
......1. Is our proposal still active? How many shifts are left? entry 580/mirror 580
......2. How can I get on site? It's my first visit/I'm arriving late or on the weekend/ I don't have a User badge. entry 602/mirror 602

467

Mon Aug 1 17:10:07 2016

8-ID-G and 8ID-E motor positions for 8ID-D mono

Att 1. shows the location of the 8-ID-D mono when working on the 8-ID-G set up.
This was a study period so ignore the gap values.

Att. 2 shows the location of the 8-ID-D mono when working on the WA-XPCS set up

Attachment 1: 8iddMono-080116.png

Attachment 2: 8iddMono-080816.png

207

Thu Oct 2 15:28:47 2008

Some misc. 8-ID-G distances (from the 8-ID-D monochromator)

- sg1 from 8-ID-D monochromator ~ 1334 mm (measured with angle offset of beam and req'd horizontal xlation of slits and known distance between sg1 and sg2 - to determine slope)
- sg2 from 8-ID-D monochromator = 1334 + 2145 = 3479 mm
- sg3 from 8-ID-D monochromator = 1334 + 2145 + 195 = 3674 mm
- diffractometer center of rotation from 8-ID-D monochromator = 1334 + 2145 + 520 = 3999 mm

Add sample-to-detector distance(s)
Add sample-to APD distance

455

Fri Apr 22 12:52:49 2016

8-ID-G initial rough alignment at 11 keV, then 8-ID-E rough alignment at 7.35 keV

This is an elog entry on the experimental commissioning of the 8-ID-G Si (111)
beamline set up at 11 keV and the return of 8-ID-E to Si (220) at 7.4 keV.
Updated drawing (April 20) are attached in attachment 4.
Ray also scanned the documents the technicians used for installation so I also
attached them to this elog as attachment 5.

On April 21, we started to line up the 8-ID-G set up with Si (111) at
11 keV. Alec wrote an update at the end of yesterday below. In brief,
with the Be window mounted directly on the 8-ID-E gate valve (GV11), we
could get a nice beam into 8-ID-E (laterally centered on the Be window) at
10.615 keV (instead of the desired 11 keV). We decided to remount the Be window
so that it is directly attached to slit sg1 as it was before we started the move
to higher energy.

On April 22, we aligned again in 8-ID-I the two undulators and monochromators.
Att. 2 shows how we aligned the DS undulator gap with respect to the
US gap set at 23.58 mm. Note the command for doing this: undgapscan dsund .
After the scan, we moved DS gap to 23.65 mm.

Att. 3 shows a 8-ID-I monochromator energy scan after this DS gap alignment.
Note that Suresh and I decided to align at slightly lower energy than 11 keV (10.96 keV)
to avoid the obvious glitch at 11.0 keV.

We then worked in 8-ID-G and centered the slit body on the beam by moving an additional 3 mm inboard.
We took burns on the exit kapton window and about 10 feet away and
then marked the floor with a red mark labelled 4/22/16 11 keV.

Scan 10 of the 8-ID-G file lineup11keV is shown in att. 1.
We went to 10.365 deg.

On 4/22 Joe, Suresh and I lined up the 8-ID-E Si (220) crystal.
Joe pointed to elog http://8id.xray.aps.anl.gov/elog/8-ID/256
for the Si (220) positions (diamz = +16.16).
We found that to pass X-rays through the center of the Be window mounted directly on the
rectangular plate mounted on the shutter, we needed to shift down the undulator energy by 120 eV.
Alec, Joe and I mounted the Be window assembly also on a JJ X-ray slit like
it was done for 8-ID-G and started to pump with the TMP overnight.

On 4/23 I was able to open the gate valve GV10, clear the EPS faults
and start preliminary alignment. I moved inboard 4.5 mm,
but I want to see where is the burn on the kapton window to see what's
going on.

The alignment was completed on 4/25. I moved back the assembly by 5 mm outboard.
This way the beam is centered on the Be window.
Att. 6 shows a diamth scan with the undulator gaps both set to 17.68 mm (usual condition).
The peak of the spectrum is at 25.7 degrees (corresponds to 7527 eV for Si (220)).
Weazel came on 4/26 to mark the floor with new red lines.

ED

Date: Thu, 21 Apr 2016 21:51:22 -0500
From: "Sandy, Alec R." <[email protected]>
To: "Dufresne, Eric" <[email protected]>,
"Narayanan, Suresh" <[email protected]>,
"Strzalka, Joseph W." <[email protected]>,
"Jiang, Zhang" <[email protected]>
Cc: "Ziegler, Raymond" <[email protected]>, "Sandy, Alec R." <[email protected]>
Subject: 8-ID-E status

Hi,

Just a quick recap of 8-ID-E�s status and suggested next steps for Friday:

* With the Be window mounted directly on the 8-ID-E gate valve (GV11), we
could get a nice beam into 8-ID-E (laterally centered on the Be window) at
10.615 keV (instead of the desired 11 keV).

* We are not sure why things don�t line up at 11 keV � probably some
uncertainty in the 8-ID-E mono position on the experiment floor. I don�t
think there is an easy way to figure out or address the origin of this
discrepancy and suggest we ignore.

*We decided to remount the Be window so that it is directly attached to slit
sg1 as it was before we started the move to higher energy. In this
configuration, there is a bellows between GV11 and the Be window so the Be
window can be translated laterally to, hopefully, accommodate the
mis-alignment mentioned above.

* We repositioned the stand holding sg1 using one hole on the floor and a
temporary clamp.

* Before venting downstream of GV11, we measured a burn on sg1. Using the
x-ray energy of ~ 10.6 keV and a desired energy of 11 keV and the distance
from the mono crystal to sg1 of 1450 mm, the beam should move 20 mm inboard
when the energy is changed to 11 keV from 10.6 keV. To center the beam in
sg1, sg1 was translated 5 mm outboard (I think). (We don�t want to go higher
than 11 keV because of absorption in the 8-ID-I monochromator at 11.1 keV.)

* We closed GV11 and vented downstream of the valve. We attached the Be
wndow to sg1 and then added the 3-3/8 bellows between the window and GV11.

* We added a pump out port on the downstream side of sg1 with a kapton
window. We left with the TMP pumping between GV11 and the Be window (with
GV11 closed) and the membrane pump pumping downstream of sg1. We moved pind1
into position by hand and attached the pind1 BNC to this pin diode. The sg1
slit aperture is 10 mm X 10 mm which are its EPICS values. The slit is
neither powered on nor connected to a serial port so can�t be opened further
unless it is connected to power and the appropriate serial connection on the
8-ID-G control rack.

* We reset the value of diamth to its value for 10.615 keV (10.7494 deg) so
there should not be a need to keep track of offsets between calculated
values of diamth and user values of diamth. They should now be the same.

Suggested To do:
* Open GV11 (assuming pressure on both sides good) and then valve off TMP
before shutting down the TMP.

* Increase energy to 11 keV in 0.1 keV steps and see if there is a signal on
pind1 (check polarity and offset as we have now switched to a different
pind1 than we were using earlier today). Iterate energy changes and diamth
scans. The peak intensity should be ~ 400,000 � 500,000 cts per sec on pind1
with the current pind1 preamp gain settings and depending obviously on the
ring current (non top-up).

* Assuming we get (or until we get) a relatively well centered beam through
the Be window and sg1 at 11 keV, take some burns along the beam path in
8-ID-E and drop these marks to the floor with a plumb bob. When we have 3 or
4, we or Weasel can add a permanent chalk mark to the floor. The dropped
marks on the floor are important but the line on the floor can wait until
convenient.

* Next would be to move onto the same for Si(220) and E=7.35 keV.

Good luck and thanks in advance for any help you can provide! Not sure how
accessible I will be tomorrow until much later in the day.

- Alec

Date: Fri, 22 Apr 2016 08:06:16 -0500
From: "Sandy, Alec R." <[email protected]>
To: "Dufresne, Eric" <[email protected]>,
"Narayanan, Suresh" <[email protected]>,
"Strzalka, Joseph W." <[email protected]>,
"Jiang, Zhang" <[email protected]>
Cc: "Ziegler, Raymond" <[email protected]>
Subject: Re: 8-ID-E status

Hi,

I did get GV11 open this am.

The other thing to add to the list assuming we get the 11 keV beam out
through the window would be to tweak one undulator relative to the other at
~ 11 keV to make sure that they are phased.

- Alec

�
Date: Fri, 22 Apr 2016 12:20:38 -0500
From: "Strzalka, Joseph W." <[email protected]>
To: "Dufresne, Eric" <[email protected]>
Cc: "Sandy, Alec R." <[email protected]>
Subject: elog on Si(220) crystal

Eric,

This Elog entry
http://8id.xray.aps.anl.gov/elog/8-ID/256 [8id.xray.aps.anl.gov]
says the diamz positions are
(111) crystal [diamz = -16.25] to the (220) crystal position [diamz =
+16.16]

Joe

--- Joseph Strzalka
Argonne National Laboratory
9700 S. Cass Ave.
�
Date: Mon, 25 Apr 2016 08:46:07 -0500
From: "Sandy, Alec R." <[email protected]>
To: "Dufresne, Eric" <[email protected]>
Subject: FW: Updated Drawing of 8-ID-D Installation
Parts/Attachments:
1 Shown ~2.1 KB Text
2 OK 1.7 MB Application, "430802-120000-UPDATED WITH CONICAL RE
----------------------------------------

- Alec

From: "Fisher, Mike V." <[email protected]>
Date: Wednesday, April 20, 2016 at 10:38
To: Alec Sandy <[email protected]>
Subject: Updated Drawing of 8-ID-D Installation

Alec:

Attached drawing has distances from downstream edge of conical reducer to
center of mono.

Mike

[ Part 2, "430802-120000-UPDATED WITH CONICAL REDUCERS.pdf" Application/PDF
(Name: "430802-120000-UPDATED WITH CONICAL REDUCERS.pdf") 1.7 MB. ]

Attachment 1: lineup11keV-scan10.png

Attachment 2: switchto11kevcommish20160421-Scan18.png

Attachment 3: switchto11kevcommish20160421-Scan19.png

Attachment 4: 430802-120000-UPDATED-WITH-CONICAL-REDUCERS.pdf

Attachment 5: D-E_flangeUpgrade2016-all.pdf

Attachment 6: linup11keV-Scan23.png

417

Fri Apr 24 12:16:44 2015

J. F. Pelletier (posted by Joe)

8-ID-G vertical focusing

I recalculated the CXRL focusing properties for 8-ID-G.

From attachment 1, I estimate the first Si (111) crystal is 51.6 m from the source.
The horizontal offset of the 8-ID-E beamline is 890 mm.
The 2Theta angle in the drawing is 31.2 degrees
so the longitudinal distance from the 1st to the second crystal is
l = 890 mm/sin(2Theta)= 1718 mm, thus the second crystal is
51600 mm + 1718 mm = 53318 mm from the source.
We measured a distance from the second crystal to the sample of 2170 mm,
so the source-experiment distance Re=55488 mm. This is an input to the calculation
code.

Calculations below are shown N=8.
Zhang used N=8 and move the lens ~100 mm downstream from the second crystal position.

It one may open up the vertical slit as you should get a smaller
spot size if we match the lens aperture to the vertical transverse coherence length.
We did measure the focus in 8-ID-E with the Optics group
http://8id.xray.aps.anl.gov/elog/8-ID/416

The best focus measure was 4.2 microns FWHM.
This is smaller than measured in 8-ID-E.
The lens vertical slit was larger than 125 microns (200 microns).

ED

What is the undulator length [m]? 2.4 m for one Und. A
The undulator length is 4.8 m
What is the photon energy? [eV]
The X-ray energy is 7350 eV
What is the material chemical formula?
The material is Be
What is the delta, the index of ref. decrement?
The real part of the index of refraction of Be is n = 1 - 6.31148e-06.
What is the X-ray absorption length (including inelastic processes)?
The X-ray absorption length is 0.00412958 m.
What is the RMS source size [m]?
The RMS source size is 1.01008e-05 m.
What is the RMS source divergence [radian]?
The RMS source divergence is 3.25712e-06 m.
What is the source to experiment distance [m]?
The source to experiment distance is 55.488 m.
What is the hole radius R [m]?
The hole radius is 0.0002 m.
What is the number of holes?
The number of holes N is 8.
What is the wall thickness between the holes [m]?
The wall thickness t is 5e-05.
What is the slit opening before the CXRL [m]?
Enter a negative number for none. N.B. Aperture must be < 2R [0.0004 m]?
You entered 0.000125.
The focal length is 1.98052 m
f = 1.98052, so = 53.4312, si = 2.05676, Re = 55.488
The RMS absorption aperture is 0.0002272 m
The RMS x-ray single electron divergence is 4.19183e-06
The RMS x-ray total divergence is 5.30851e-06
The lens radius of curvature is 0.0002 m
The magnification is 0.0384935 (25.9784:1)
The RMS beamsize before the lens is 0.00028382 m
The RMS beamsize after the lens is 0.000177369 m
The FWHM beamsize at the experiment without the lens is 0.00069262 m
The FWHM diff. limit. spot size is 2.45901e-06 m
The FWHM image size is 2.62329e-06 m
The wall transmission is 0.907681
The theoretical gain is 77.734
Spherical aberration matter for r > 8.55056e-05 [m]
This number is useful for cylindrical lenses
The transverse coherence length in the plane of the lens is 0.000251718

Attachment 1: 8ID-D-Mono-Position.png

Attachment 3: GISAXS-slits-0422.png

237

Mon Jul 27 14:07:56 2009

8-ID-I Layout information from IMMY-XOR webpage

Other

[The attached information about the layout of the 8-ID-I hutch was previously posted on the IMMY-XOR webpage under User Info/Layout/Sector 8
/I]

8-ID XOR - Layout

8-ID XOR 8-ID-I Hutch

Hutch 8-ID-I is the end station dedicated to the COSAXS setup. A side station for micro-diffraction
can also be setup in this hutch.

DWG (118K) EPS (582K) Hutch layout

Some pictures:

Outside
Inside

J. F. Pelletier
June 2000

Attachment 1: 8-ID-I_XOR_-_Layout.mht

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Attachment 2: 8IDI_layout.dwg

Attachment 3: 8IDI_layout.ps

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8-ID-I